Method for analysis of heavy sulphur compounds using gas chromatography with flame photometric detection

N. Moreira; P. Guedes De Pinho; I. Vasconcelos

doi:10.1016/j.aca.2003.12.041

Method for analysis of heavy sulphur compounds using gas chromatography with flame photometric detection

N. Moreira, P. Guedes De Pinho, I. Vasconcelos^*

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

13 Citations (Scopus)

223 Downloads

Abstract

A method for analysis of heavy sulphur compounds in wines, based on gas chromatography (GC) with flame photometric detection, is reported. Wine samples preparation includes a dichloromethane liquid-liquid extraction followed by concentration under a nitrogen atmosphere. The extracted fraction was also analysed by GC-mass spectrometry. The method enables high recovery of sulphur compounds in wine and satisfies the requirements of repeatability and sensitivity. Applications of the method to red, white and Port wines are reported.

Original language	English
Title of host publication	Papers presented at the 3rd Symposium In Vino Analytica Scientia Aveiro, Portugal, 10-12 July 2003
Pages	183-189
Number of pages	7
Volume	513
Edition	1
DOIs	https://doi.org/10.1016/j.aca.2003.12.041
Publication status	Published - 18 Jun 2004
Event	3rd Symposium In Vino Analytica Scientia Aveiro - Aveiro, Portugal Duration: 10 Jul 2003 → 12 Jul 2003 Conference number: 3

Publication series

Name	Analytica Chimica Acta
Publisher	Elsevier
ISSN (Print)	0003-2670

Conference

Conference	3rd Symposium In Vino Analytica Scientia Aveiro
Country/Territory	Portugal
City	Aveiro
Period	10/07/03 → 12/07/03

Keywords

Flame photometric detection
Gas chromatography
Sulphur compounds
Wine

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10.1016/j.aca.2003.12.041

19694305Accepted author manuscript, 120 KBLicence: CC BY-NC-ND

http://hdl.handle.net/10400.14/3510Licence: CC BY-NC-ND

Cite this

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title = "Method for analysis of heavy sulphur compounds using gas chromatography with flame photometric detection",

abstract = "A method for analysis of heavy sulphur compounds in wines, based on gas chromatography (GC) with flame photometric detection, is reported. Wine samples preparation includes a dichloromethane liquid-liquid extraction followed by concentration under a nitrogen atmosphere. The extracted fraction was also analysed by GC-mass spectrometry. The method enables high recovery of sulphur compounds in wine and satisfies the requirements of repeatability and sensitivity. Applications of the method to red, white and Port wines are reported.",

keywords = "Flame photometric detection, Gas chromatography, Sulphur compounds, Wine",

author = "N. Moreira and {Guedes De Pinho}, P. and I. Vasconcelos",

year = "2004",

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doi = "10.1016/j.aca.2003.12.041",

language = "English",

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series = "Analytica Chimica Acta",

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booktitle = "Papers presented at the 3rd Symposium In Vino Analytica Scientia Aveiro, Portugal, 10-12 July 2003",

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note = "3rd Symposium In Vino Analytica Scientia Aveiro ; Conference date: 10-07-2003 Through 12-07-2003",

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Moreira, N, Guedes De Pinho, P & Vasconcelos, I 2004, Method for analysis of heavy sulphur compounds using gas chromatography with flame photometric detection. in Papers presented at the 3rd Symposium In Vino Analytica Scientia Aveiro, Portugal, 10-12 July 2003. 1 edn, vol. 513, Analytica Chimica Acta, pp. 183-189, 3rd Symposium In Vino Analytica Scientia Aveiro, Aveiro, Portugal, 10/07/03. https://doi.org/10.1016/j.aca.2003.12.041

Method for analysis of heavy sulphur compounds using gas chromatography with flame photometric detection. / Moreira, N.; Guedes De Pinho, P.; Vasconcelos, I.
Papers presented at the 3rd Symposium In Vino Analytica Scientia Aveiro, Portugal, 10-12 July 2003. Vol. 513 1. ed. 2004. p. 183-189 (Analytica Chimica Acta).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Method for analysis of heavy sulphur compounds using gas chromatography with flame photometric detection

AU - Moreira, N.

AU - Guedes De Pinho, P.

AU - Vasconcelos, I.

N1 - Conference code: 3

PY - 2004/6/18

Y1 - 2004/6/18

N2 - A method for analysis of heavy sulphur compounds in wines, based on gas chromatography (GC) with flame photometric detection, is reported. Wine samples preparation includes a dichloromethane liquid-liquid extraction followed by concentration under a nitrogen atmosphere. The extracted fraction was also analysed by GC-mass spectrometry. The method enables high recovery of sulphur compounds in wine and satisfies the requirements of repeatability and sensitivity. Applications of the method to red, white and Port wines are reported.

AB - A method for analysis of heavy sulphur compounds in wines, based on gas chromatography (GC) with flame photometric detection, is reported. Wine samples preparation includes a dichloromethane liquid-liquid extraction followed by concentration under a nitrogen atmosphere. The extracted fraction was also analysed by GC-mass spectrometry. The method enables high recovery of sulphur compounds in wine and satisfies the requirements of repeatability and sensitivity. Applications of the method to red, white and Port wines are reported.

KW - Flame photometric detection

KW - Gas chromatography

KW - Sulphur compounds

KW - Wine

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U2 - 10.1016/j.aca.2003.12.041

DO - 10.1016/j.aca.2003.12.041

M3 - Conference contribution

AN - SCOPUS:2442551715

VL - 513

T3 - Analytica Chimica Acta

SP - 183

EP - 189

BT - Papers presented at the 3rd Symposium In Vino Analytica Scientia Aveiro, Portugal, 10-12 July 2003

T2 - 3rd Symposium In Vino Analytica Scientia Aveiro

Y2 - 10 July 2003 through 12 July 2003

ER -

Method for analysis of heavy sulphur compounds using gas chromatography with flame photometric detection

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Keywords

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